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User name kramerk
Log entry time 01:25:10 on July24,2001
Entry number 67337
keyword=Target - NMR/EPR - 45.0%/44.1%
Conditions: 3 lasers on, no gradient field, holding field @ 180 deg., pick-up coils position.
00:44 - Asked MCC to mask the Target FSD
00:45 - Moved Target into pick-up coils position
00:48 - Performed NMR
00:50 - Failed EPR. RF field did not turn on. There was no change in the resonance. I waited until the sweep trigger was finished. During this time the green light on the HP FG did not come on. I assumed it was a communications problem. I stopped the EPR VI. I put the HP FG in local and reset the amplitude to 0.4 V rms and turned the FG on.
00:54 I tried to do another sweep, but now the EPR VI is not reading the SRS620 counter. I assume its a LabVIEW problem and exit LabView and reenter the TO screen and start the EPR AFP VI again.
00:58 Perform a successful EPR measurement!
01:00 Moved target back in to Pol. 3He position
LabVIEW extraction of NMR signal - 45.0%
EPR fits using Xiaochao's code:
0th order fit:
down: freq. shift = -49.14 KHz +/- 1.79 KHz, P = -44.88%+/- 1.63%
up: freq. shift = 47.65 KHz +/- 1.64 KHz, P = 43.52%+/- 1.50%
1st order fit:
down: freq. shift = -48.23 KHz +/- 1.74 KHz, P = -44.04%+/- 1.59%
up: freq. shift = 48.19 KHz +/- 1.62 KHz, P = 44.01%+/- 1.48%
comments: final EPR looks good! Holding field a little lower than previous EPR.