Difference between revisions of "Thermal Equilibrium Measurement Procedure"
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(New page: ;This procedure was created for GEN, and must be updated to reflect changes in the target for g2p. ===Assumptions:=== *NMR System is tuned *Magnet is at full field, persistent mode, leads...) |
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;This procedure was created for GEN, and must be updated to reflect changes in the target for g2p. | ;This procedure was created for GEN, and must be updated to reflect changes in the target for g2p. | ||
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+ | TO aid in the TE calculation, use the "te_getter.pl" script in the g2p_te folder on poltarg2p2. | ||
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+ | Changes for g2p: Set the run valve to a reasonable value, close to the setpoint chosen by the PID. 65% to 90% is a bit too much for this fridge. | ||
===Assumptions:=== | ===Assumptions:=== |
Revision as of 17:08, 28 February 2012
- This procedure was created for GEN, and must be updated to reflect changes in the target for g2p.
TO aid in the TE calculation, use the "te_getter.pl" script in the g2p_te folder on poltarg2p2.
Changes for g2p: Set the run valve to a reasonable value, close to the setpoint chosen by the PID. 65% to 90% is a bit too much for this fridge.
Assumptions:
- NMR System is tuned
- Magnet is at full field, persistent mode, leads are ramped down
- Nose is full, run valve in manual mode
Prepare Fridge:
- Stop RB3, RB2, and RB1 (wait 2 mintues between each), if necessary
- Put Run Valve, EV91120, in Manual Mode
- Establish a STEADY Nose level somewhere between 65% and 90%
- Only make slight changes to Run Valve for rest of TE (+/- 0.05 each 10 min)
Take a Baseline:
- Hit "Unlock Magnet Controls" button
- Type the full-field current in the box labeled "Setpoint" (eg: 77.085)
- Type 0.50 into "Setrate" box, if necessary
- Hit "To Setpoint" Button
- Wait for leads to reach full current (approx 1 min)
- Hit "Hold"
- Check that leads current and magnet current are equal
- Hit "Heater On" button
- Wait for the 30 second timeout to expire
- Type the baseline current into the "Setpoint" box (eg: 74.600)
- Hit "To Setpoint" to start the magnet sweeping
- Wait for magnet to reach baseline current (approx 6 min)
- Hit "Hold" button
- Put NMR into pause mode if necessary
- Hit the Baseline button
- Select "Create New Baseline", dialog box should then disappear
- Change sweeps to 5000 if necessary
- Double check that all NMR settings are where you want them
- Hit "One Point" button to take a single nmr measurement
- Wait for timer to count down
- Hit Baseline button
- Select the baseline you just took from the list of timestamps
- Document the details of the baseline in the logbook:
- Date Time, #Sweeps, MagCurrent, Top/Bottom, Gain, RFFreq, RFMod
- Type full-field current into "Setpoint" box (eg: 77.085)
- Type 0.50 into "Setrate" box, if necessary
- Hit "To Setpoint" button
- Wait for magnet to reach full current (approx 6 min)
- Hit "Hold" button
- Hit "Heater Off" button
- Wait for 30 second timeout to expire
- Hit "To Zero" to ramp the leads down
- Hit "Lock Magnet Controls" button
Take TE measurements:
- Make sure ladder is in desired target position
- Make sure NMR is on desired channel (AND in agreement with target position!)
- Set sweeps to 5000, if necessary
- Hit "Take Data" button
- Wait for timer to count down
- Write the following in the logbook for the next 10 measurements:
- Time, NMR Area, 4He Press, 4He Temp, 3He Press, 3He Temp, Nose Level