After this has been determined I will be able to go back to the EPR calibrations. I already have the knowledge to adjust the temperature of the cell. I will separate out the EPR calibrations into the two spin states, and separate out each spin state into ``equilibrium states''. Then I will be able to assign a calibration number (with somewhat reasonable error) to be applied to all NMR measurements.
There will still be room for improvement in terms of improving the fit and making sense of the data for the other cells, but within the next four weeks I believe I will have acceptable polarization numbers for the last kinematic point.